Zu Hanser-Fachbuch.de
Warenkorb
Alberto Naranjo C., María del Pilar Noriega E., Tim A. Osswald, Alejandro Roldán-Alzate, Juan Diego Sierra M.
Plastics Testing and Characterization
Industrial Applications
PREFACE
8
TABLE OF CONTENTS
10
CHAPTER 1: INTRODUCTION
14
1.1 TESTING TECHNIQUES
14
1.2 STEPS FOR SUCCESSFUL POLYMER CHARACTERIZATION
17
1.3 PREPARATION AND SEPARATION TECHNIQUES
17
References
19
CHAPTER 2: SPECTROSCOPY
20
2.1 FTIR SPECTROSCOPY
21
2.1.1 FTIR Spectrophotometer
22
2.1.2 FTIR Techniques
24
2.1.3 Correlation of Polymer and Additives Structure and FTIR Spectra
27
2.1.4 Useful FTIR Standard Measuring Techniques
33
2.2 RAMAN SPECTROSCOPY
58
2.3 ENERGY DISPERSIVE X-RAY SPECTROSCOPY
64
References
66
CHAPTER 3: GAS CHROMATOGRAPHY AND SELECTIVE MASS DETECTION
68
3.1 GAS CHROMATOGRAPHY INSTRUMENTATION
68
3.2 CORRELATION OF ADDITIVE STRUCTURE AND MASS SPECTRA
72
3.3 SELECTED STANDARDS FOR GAS CHROMATOGRAPHY TESTING
75
References
86
CHAPTER 4: THERMAL PROPERTIES
88
4.1 THERMAL CONDUCTIVITY
88
4.2 SPECIFIC HEAT AND SPECIFIC ENTHALPY
93
4.3 DENSITY
97
4.4 THERMAL DIFFUSIVITY
97
4.4.1 New Developments in Thermal Diffusivity Measurement
101
4.5 LINEAR COEFFICIENT OF THERMAL EXPANSION
104
4.6 CURING BEHAVIOR
110
4.7 THERMAL ANALYSIS AND MEASURING DEVICES
113
4.7.1 Differential Scanning Calorimetry (DSC)
115
4.7.2 Thermogravimetry (TGA)
133
References
139
CHAPTER 5: MELT RHEOLOGY
140
5.1 BASIC CONCEPTS AND TERMINOLOGY
141
5.2 CONSTITUTIVE MODELS
155
5.2.1 Newtonian Model
156
5.2.2 Power Law Model
156
5.2.3 Bird-Carreau-Yasuda Model
157
5.2.4 Pressure Dependence of Viscosity
158
5.2.5 Phan-Thien and Tanner Multimode Model
159
5.3 RHEOMETRY
160
5.3.1 The Melt Flow Indexer
160
5.3.2 Capillary Viscometer
163
5.3.3 Rotational Rheometry
170
5.3.4 Extensional or Elongational Rheometry
178
References
196
CHAPTER 6: MECHANICAL PROPERTIES
198
6.1 MECHANICAL PROPERTIES
198
6.1.1 The Short-Term Tensile Test
198
6.1.2 Impact Strength
213
6.1.3 Creep Behavior
238
6.1.4 Dynamic Mechanical Tests
254
6.1.5 Fatigue Tests
259
6.1.6 Strength Stability Under Heat
266
References
273
CHAPTER 7: PERMEABILITY PROPERTIES
276
7.1 SORPTION
277
7.2 DIFFUSION AND PERMEATION
278
7.3 MEASURING S, D, AND P
288
7.4 DIFFUSION OF POLYMER MOLECULES AND SELF-DIFFUSION
294
References
298
CHAPTER 8: ENVIRONMENTAL EFFECTS AND AGING
300
8.1 WATER ABSORPTION
300
8.2 WEATHERING
304
8.3 CHEMICAL DEGRADATION
314
8.4 THERMAL DEGRADATION OF POLYMERS
321
References
327
CHAPTER 9: ELECTRICAL, OPTICAL, AND ACOUSTIC PROPERTIES
328
9.1 ELECTRICAL PROPERTIES
328
9.1.1 Dielectric Behavior
328
9.1.2 Electric Conductivity
334
9.1.3 Application Problems
339
9.1.4 Magnetic Properties
351
9.2 OPTICAL PROPERTIES
352
9.2.1 Index of Refraction
353
9.2.2 Photoelasticity and Birefringence
355
9.2.3 Transparency, Reflection, Absorption, and Transmittance
357
9.2.4 Gloss
362
9.2.5 Color
364
9.3 ACOUSTIC PROPERTIES
366
9.3.1 Speed of Sound
367
9.3.2 Sound Reflection
367
9.3.3 Sound Absorption
368
References
370
INDEX
372
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